The module aims to provide the students with: a knowledge of analytical measurement systems, theory of chromatographic methods, HPLC and GC techniques; the ability to carry out simple quantitative and qualitative analysis; the ability to apply chromatographic techniques to analytical laboratory environments; knowledge of forensic sample collection procedures including forensic photography and basic characteristics of forensic samples with a focus on arson and explosives.
Evidence Collection and Search Methods
Sampling Practice Guidelines; Sample Composition, Collection Protocols, Kits and Storage - Fibres, Paint, Glass, Toolmarks, Footwear and Tyre Mark Impressions, Firearms Residue, Biological Fluids, Drugs, Arson, Explosives. The Crime Scene; Search Methods; Registering the scene (including Video and photographic aspects) Chemical Enhancement Techniques; Sample Pre-treatment for Analysis.
Chromatographic methods
Classification / Chromatograms / Chromatographic behaviour of solutes / Efficency and Resolution / Qualitative & Quantitative analysis (internal and external standards);
Introduction to HPLC
Instrumental layout / Pumps / Gradients vs. Isocratic / Sample Injectors / Tubing and Connections / Pre- and Analytical Columns / Standard Detectors / Separation Modes (Size Exclusion, Ion Exchange, Speciality, Normal Phase and Reverse Phase) / Polarity / Column Ovens / Solvents / Trouble shooting / Sample Preparation (filtration, liquid-liquid extraction, Solid Phase Extraction);sample preparation; elution; column classification; detectors; trouble-shooting.
Introduction to GC
System / Components / Separation sequence / Injection Port / Columns (Packed and Capillary) / Oven (temp. programming) / Standard Detectors / Qualitative & Quantitative analysis (response Factors) / Trouble-shooting.
Lecture-based instruction - Traditional Lectures; Small group work, Digital Learning
Individual learning - Small group work, Digital Learning
| Module Content & Assessment | |
|---|---|
| Assessment Breakdown | % |
| Formal Examination | 70 |
| Other Assessment(s) | 30 |